Determination of blood lead by electron-capture negative chemical ionization gas chromatography-mass spectrometry

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Determination of blood lead by electron-capture negative chemical ionization gas chromatography-mass spectrometry.

An electron-capture negative chemical ionization (NCI) gas chromatography-mass spectrometry (GC-MS) method for determination of lead (Pb) in blood samples is described. Extraction of Pb from the sample does not involve hot digestion but is based on treatment at ambient temperature. The blood sample is supplemented with a known amount of internal standard (204Pb) for isotope dilution and is trea...

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ژورنال

عنوان ژورنال: Clinical Chemistry

سال: 1996

ISSN: 0009-9147,1530-8561

DOI: 10.1093/clinchem/42.2.286